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Plos One : 13C-13C Homonuclear Recoupling in Solid-state Nuclear Magnetic Resonance at a Moderately High Magic-angle- Spinning Frequency, Volume 7

By Pastore, Annalisa

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Book Id: WPLBN0003932588
Format Type: PDF eBook :
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Reproduction Date: 2015

Title: Plos One : 13C-13C Homonuclear Recoupling in Solid-state Nuclear Magnetic Resonance at a Moderately High Magic-angle- Spinning Frequency, Volume 7  
Author: Pastore, Annalisa
Volume: Volume 7
Language: English
Subject: Journals, Science, Medical Science
Collections: Periodicals: Journal and Magazine Collection (Contemporary)
Historic
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Publisher: Plos

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Pastore, A. (n.d.). Plos One : 13C-13C Homonuclear Recoupling in Solid-state Nuclear Magnetic Resonance at a Moderately High Magic-angle- Spinning Frequency, Volume 7. Retrieved from http://netlibrary.net/


Description
Description : Two-dimensional 13C-13C correlation experiments are widely employed in structure determination of protein assemblies using solid-state nuclear magnetic resonance. Here, we investigate the process of 13C-13C magnetisation transfer at a moderate magic-angle-spinning frequency of 30 kHz using some of the prominent second-order dipolar recoupling schemes. The effect of isotropic chemical-shift difference and spatial distance between two carbons and amplitude of radio frequency on 1H channel on the magnetisation transfer efficiency of these schemes is discussed in detail.

 

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